Beilstein J. Org. Chem.2022,18, 446–458, doi:10.3762/bjoc.18.47
-fluoro-N-hydroxybenzimidoyl chloride (1a) and 1-phenylbutane-1,3-dione (2a) (Table 1) as the starting materials and a water–methanol mixture as the aqueousreactionmedium. A series of organic and inorganic bases was screened at room temperature in various combinations of water–methanol mixtures and
Beilstein J. Org. Chem.2017,13, 1717–1727, doi:10.3762/bjoc.13.166
make this protocol a great option for stilbene syntheses by Mizoroki–Heck reaction.
Keywords: aqueousreactionmedium; MAOS; Mizoroki–Heck reaction; Pd nanoparticle; sustainable organic synthesis; Introduction
Palladium-catalyzed reactions have emerged as an important tool for organic synthesis
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Graphical Abstract
Scheme 1:
Synthesis of (E)-pterostilbene (19) catalyzed by PVP-Pd NPs.